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7-Gallon Bourbon Mash Recipe (Classic Small-Batch Style)

7-Gallon Bourbon Mash Recipe (Classic Small-Batch Style)
Mash Bill:
- 78% corn
- 12% malted barley
- 10% malted rye
Yeast:
- Fleischmann’s All-Grain Yeast (or any quality distiller’s yeast)
1. Calculate Your Grain Amounts
For a 7-gallon mash, use a ratio of roughly 2 pounds of grain per gallon of water.
| Grain | Percentage | Weight |
|---|---|---|
| Corn | 78% | 10.9 lbs |
| Malted Barley | 12% | 1.7 lbs |
| Malted Rye | 10% | 1.4 lbs |
| Total Grain | 100% | 14 lbs |
2. Mashing Process
Step 1 — Heat & Add Corn:
- Heat 4 gallons of water to 190–200°F (88–93°C).
- Gradually stir in the cracked corn, ensuring there are no dry clumps.
- Maintain this temperature for 90 minutes, stirring often to avoid scorching.
This step gelatinizes the corn starch so it can later convert into sugar.
Step 2 — Add Malted Grains:
- Cool the mash to 150–160°F (65–71°C).
- Add malted barley and malted rye, which provide the enzymes needed for starch-to-sugar conversion.
Step 3 — Saccharification Rest:
- Keep the mash between 147–152°F (64–67°C) for 60–90 minutes.
- Stir occasionally.
- Test with iodine: if the test shows no black/blue color, starch conversion is complete.
Step 4 — Mash Out:
- Raise temperature to 170°F (77°C) for 10–20 minutes to halt enzyme activity and improve sugar extraction.
3. Fermentation
Step 1 — Cool & Transfer:
- Chill the mash to 70–77°F (21–25°C).
- Transfer into a sanitized fermenter.
Step 2 — Add Yeast (and Optional Backset):
- Pitch your yeast and add a yeast nutrient if desired.
- Optionally, add backset (liquid left from a previous distillation) at a ratio of 1:3 or 1:4 to stabilize pH and enhance flavor.
Step 3 — Ferment:
- Seal the fermenter with an airlock.
- Let it ferment for 5–7 days (or until bubbling slows).
- The mash should finish with a mildly sweet, sour aroma and an alcohol content around 8–10%.
4. Distillation & Aging
Step 1 — Distill:
- Run the fermented mash through a pot still or reflux still, discarding foreshots responsibly.
- Collect the distillate in stages to separate heads, hearts, and tails.
Step 2 — Age:
- Transfer the heart cut into new, charred American oak barrels.
- Age for at least 2 years to produce a straight bourbon, or longer for deeper caramel and vanilla notes.
Notes
- Temperature control and sanitation are key at every step.
- Experiment with yeast strains and aging times to develop your signature flavor.
- Label and store barrels in a cool, stable environment for optimal aging.



